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Beilstein J. Org. Chem. 2021, 17, 379–384, doi:10.3762/bjoc.17.33
Graphical Abstract
Scheme 1: The continuous flow set-up used.
Figure 1: Scope of Cbz-carbamate products obtained via flow process (*tRes = 60 min, **T = 80 °C; isolated yi...
Scheme 2: Side reaction during formation of product 3m.
Scheme 3: Flow set-up for the CALB-mediated impurity tagging approach.
Scheme 4: Strategies towards accessing β-amino acid derivatives 8.
Scheme 5: Complementary flow approaches towards the β-amino acid derivatives 8.
Scheme 6: Batch hydrolysis of the ester group in the presence of the carbamate.